High Temperature oxidation evaluation using crystal microbalance - IFPEN - IFP Energies nouvelles Accéder directement au contenu
Article Dans Une Revue Corrosion Engineering, Science and Technology Année : 2020

High Temperature oxidation evaluation using crystal microbalance

Résumé

High-temperature oxidising environments are frequently encountered but the limited number of in situ techniques that can be implemented has hindered the monitoring possibilities and a better comprehension of the oxidation phenomenon. In this paper the high temperature oxidation behaviours of three alloys (AISI 316L, AISI 310 and HAYNES ® HR-120 ®) were studied by using crystal microbalances and surface characterizations. For the microbalance experiments two types of crystal were tested: quartz or gallium orthophosphate crystals. First the behaviour of thin sputtered deposited alloys on quartz slides was studied at 400 and 700°C under air oxidising conditions and compared to bulk samples. Kinetics measurements were performed on the three alloy films deposited on the resonators at 400 or 700°C under air. After the calibration of quartz and gallium orthophosphate crystals, it was possible to measure very small mass variations associated with thin oxide formation between 5 and 180 nm of thickness. The crystal microbalance technique gives very promising perspectives in understanding the high-temperature corrosion and scaling mechanisms and also for in situ monitoring.

Domaines

Matériaux
Fichier principal
Vignette du fichier
CST3722.pdf (1.12 Mo) Télécharger le fichier
Origine Fichiers produits par l'(les) auteur(s)
Loading...

Dates et versions

hal-02539436 , version 1 (10-04-2020)

Identifiants

Citer

Michael Nicoli, François Grosjean, Rémy Mingant, Jean Kittel, Monica Trueba, et al.. High Temperature oxidation evaluation using crystal microbalance. Corrosion Engineering, Science and Technology, 2020, 55 (5), pp.365-371. ⟨10.1080/1478422X.2020.1732122⟩. ⟨hal-02539436⟩
102 Consultations
139 Téléchargements

Altmetric

Partager

Gmail Mastodon Facebook X LinkedIn More